Litcius/Paper detail

Palladium-Catalyzed Ring-Opening Reaction of Cyclopropenones with Vinyl Epoxides

Liguo Lu, Junhua Chen, Xiaobo Huang, Miaochang Liu, Yunbing Zhou, Huayue Wu

2022The Journal of Organic Chemistry10 citationsDOI

Abstract

We report herein the Pd-catalyzed selective ring-opening reaction of cyclopropenones with vinyl epoxides. By using a commercially available Pd2(dba)3·CHCl3–BINAP catalyst, a wide range of conjugated alkadienyl carboxylates could be accessed in good yield and excellent regioselectivity. The new application of zwitterionic π-allyl palladium intermediates has been demonstrated in organic synthesis.

Topics & Concepts

ChemistryRegioselectivityPalladiumCatalysisRing (chemistry)Yield (engineering)Conjugated systemEpoxideOrganic chemistryCombinatorial chemistryPolymer chemistryMaterials scienceMetallurgyPolymerCyclopropane Reaction MechanismsCatalytic Alkyne ReactionsSynthetic Organic Chemistry Methods