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A Theoretical Model for Computing Freezing Point Depression of Lithium-Ion Battery Electrolytes

Julian Self, Helen K. Bergstrom, Kara D. Fong, Bryan D. McCloskey, Kristin A. Persson

2021Journal of The Electrochemical Society14 citationsDOIOpen Access PDF

Abstract

Reliable prediction of freezing point depression in liquid electrolytes will accelerate the development of improved Li-ion batteries which can operate in low temperature environments. In this work we establish a computational methodology to calculate activity coefficients and liquidus lines for battery-relevant liquid electrolytes. Electronic structure methods are used in conjuction with classical molecular dynamics simulations and theoretical expressions for Born solvation energy, ion-atmosphere effects from Debye-Hückel theory and solvent entropic effects. The framework uses no a priori knowledge beyond neat solvent properties and the concentration of salt. LiPF 6 in propylene carbonate (PC), LiPF 6 in dimethyl carbonate (DMC) and LiClO 4 in DMC are investigated up to 1 molal with accuracy better than 3 °C when compared to experimental freezing point measurements. We find that the difference in freezing point depression between the propylene carbonate-based electrolyte and the dimethyl carbonate electrolytes originates from the difference in the solvent dielectric constant.

Topics & Concepts

Freezing-point depressionElectrolytePropylene carbonateSolvationChemistryFreezing pointMolalitySolventThermodynamicsBattery (electricity)Inorganic chemistryLiquidusDimethoxyethaneDimethyl carbonatePhysical chemistryOrganic chemistryAqueous solutionPhysicsElectrodeMethanolPower (physics)AlloyAdvanced Battery Materials and TechnologiesIonic liquids properties and applicationsThermodynamic properties of mixtures
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