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Elemental Sulfur-Mediated Synthesis of Quinoxalines from Sulfoxonium Ylides

Trayambek Nath Chaubey, Paran J. Borpatra, Satyendra Kumar Pandey

2023Organic Letters33 citationsDOI

Abstract

A novel straightforward and catalyst-free approach for synthesizing quinoxaline derivatives from sulfoxonium ylides and o -phenylenediamines mediated by elemental sulfur has been described. Due to the simple and mild reaction conditions, the sulfoxonium ylides and o -phenylenediamines decorated with different functional groups furnished moderate to high yields of quinoxaline derivatives and were well tolerated. Finally, large-scale reactions, the synthesis of pyrazines, and some bioactive compounds are used to illustrate the potential utility of the developed approach.

Topics & Concepts

QuinoxalineChemistrySulfurCatalysisCombinatorial chemistryOrganic chemistryReaction conditionsSynthesis and Biological EvaluationSulfur-Based Synthesis TechniquesCyclopropane Reaction Mechanisms
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