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Ostwald ripening leads to less hysteresis during hydrogen injection and withdrawal: A pore-scale imaging study

Sepideh Goodarzi, Guanglei Zhang, Branko Bijeljic, Martin J. Blunt

2025International Journal of Hydrogen Energy16 citationsDOIOpen Access PDF

Abstract

This study explores hydrogen storage in Bentheimer sandstone using high-resolution 3D X-ray imaging during hydrogen injection and brine flooding cycles. The results reveal a reduction in hysteresis during hydrogen injection and withdrawal, attributed to Ostwald ripening–the transport of dissolved hydrogen in the aqueous phase to balance local capillary pressure. Hydrogen saturation reached 82% after injection, while the residual saturation decreased significantly from 40% in the first cycle of brine injection (imbibition) to less than 18% in the third. End-point capillary pressure during gas injection was directly measured as 20, 9, and 3 kPa in the first, second, and third cycles, respectively. During the imbibition steps, the gas saturation decreased consistently, reflecting reduced trapping effects and improved gas connectivity. After 16 h of rest, a single large connected ganglion formed, further reducing the Euler characteristic per unit volume from -10 mm − 3 to -23 mm − 3 during the third drainage cycle. These findings highlight that traditional hysteresis models that ignore the effect of Ostwald ripening over-estimate the amount of residual trapping in hydrogen storage. • A porous plate drainage experiment, resulted in an average hydrogen saturation of 82%. • Capillary pressure was as 20, 9, and 3 kPa for drainage during 3 injection cycles. • A 16 h no-flow period improved gas connectivity, forming a single connected ganglion. • Gas redistribution via Ostwald ripening, occurred without altering the overall volume. • Repeated drainage-imbibition cycles reduced residual saturation from 40% to 18%.

Topics & Concepts

Ostwald ripeningHysteresisRipeningHydrogenMaterials scienceScale (ratio)ThermodynamicsChemistryNanotechnologyPhysicsCondensed matter physicsOrganic chemistryFood scienceQuantum mechanicsHydrogen embrittlement and corrosion behaviors in metalsEnhanced Oil Recovery TechniquesMetallurgical Processes and Thermodynamics
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