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A Model System for Photocatalysis: Ti-Doped α-Fe<sub>2</sub>O<sub>3</sub>(1102) Single-Crystalline Films

Giada Franceschi, Florian Kraushofer, Matthias Meier, Gareth S. Parkinson, Michael Schmid, Ulrike Diebold, Michele Riva

2020Chemistry of Materials20 citationsDOIOpen Access PDF

Abstract

(11̅02) films by pulsed laser deposition (PLD). We characterize their surfaces, combining in situ scanning tunneling microscopy (STM) with density functional theory (DFT), and reveal how dilute Ti impurities modify the atomic-scale structure of the surface as a function of the oxygen chemical potential and Ti content. Ti preferentially substitutes subsurface Fe and causes a local restructuring of the topmost surface layers. Based on the experimental quantification of Ti-induced surface modifications and the structural model we have established, we propose a strategy that can be used to separate the effects of Ti-induced modifications to the surface atomic and electronic structures and bulk conductivity on the reactivity of Ti-doped hematite.

Topics & Concepts

Materials scienceDopingHematitePulsed laser depositionConductivityWater splittingNanotechnologyDensity functional theoryImpurityScanning tunneling microscopeChemical engineeringPhotocatalysisChemical physicsThin filmOptoelectronicsPhysical chemistryChemistryComputational chemistryCatalysisMetallurgyOrganic chemistryBiochemistryEngineeringIron oxide chemistry and applicationsMicrobial Fuel Cells and BioremediationRadioactive element chemistry and processing