Testing of liquids with the cone calorimeter
Matthew J. DiDomizio, Vusal Ibrahimli, Elizabeth J. Weckman
Abstract
The cone calorimeter is traditionally used to measure the response of solid materials to radiant heating. Liquids are also commonly tested, but the methods employed are varied and inconsistent. There is a need to understand how the experimental conditions impact test results, and to develop formal guidance on a testing protocol for liquids. The cone calorimeter can be used to characterize the fire performance of liquids according to their propensities for ignition, boiling, and burning, as well as their combustion characteristics. A review of the literature was carried out to understand the breadth of apparatus and procedures used to date and their impacts on test results. From this, a series of recommendations were developed for adapting the test protocol for liquids. The vessel used should be circular; steel, borosilicate glass, or fused quartz; positioned on 13 mm of flat ceramic fiber insulation within a larger spillage containment pan; and have a diameter between 65 mm and 90 mm. Liquid depths of 10 mm should be used, and tests should be nominally be conducted at a heat flux of 10 kW⋅m−2. This work provides the necessary technical basis for adoption of a consistent methodology for cone calorimeter testing of liquids.