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Green synthesis of PVC/ZnO nanoparticles: microstructure, thermal properties, optical behavior, radiation shielding efficiency, and mechanical performance

Hakan Yaykaşlı, Hasan Eskalen, Mustafa Kavgacı, Hacı Veli Kalmış

2025Materials Science and Engineering B14 citationsDOIOpen Access PDF

Abstract

This research details a sustainable, green synthesis of ZnO nanoparticles (ZnO-NPs) using Capsicum annuum L. (pepper) extract and their incorporation into a polyvinyl chloride (PVC) matrix to fabricate high-performance nanocomposite films. Characterization confirmed the formation of hexagonal wurtzite ZnO-NPs with an average crystallite size of 10–20 nm, which were homogeneously dispersed within the PVC matrix. The inclusion of ZnO-NPs significantly enhanced the material’s properties. Thermal stability improved, with the degradation onset temperature increasing from 343 °C to 350 °C. Mechanically, tensile strength rised 60 to 75 N, and elongation at break more than doubled from 6 % to 13 %. Optical analysis revealed a reduction in the material’s direct band gap from 5.13 to 5.07 eV. Furthermore, radiation shielding capabilities were bolstered, evidenced by an increased LAC (from 0.133 to 0.143 cm −1 ). This work presents an eco-friendly method for developing multifunctional PVC nanocomposites with promising applications in advanced biomedical and nuclear fields.

Topics & Concepts

MicrostructureMaterials scienceRadiation shieldingElectromagnetic shieldingNanoparticleComposite materialThermalRadiationIrradiationNanotechnologyOpticsMeteorologyNuclear physicsPhysicsPolymer Nanocomposite Synthesis and IrradiationRadiation Shielding Materials AnalysisPolymer Nanocomposites and Properties
Green synthesis of PVC/ZnO nanoparticles: microstructure, thermal properties, optical behavior, radiation shielding efficiency, and mechanical performance | Litcius