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Rh(III)‐Catalyzed C−H Functionalization of <i>N‐</i>Nitrosoanilines with <i>α</i>‐Sulfonylcarbenes

Rui‐jun Peng, Lei Chen, Xue‐Jing Zhang, Ming Yan

2022Advanced Synthesis & Catalysis13 citationsDOI

Abstract

Abstract A Rh(III)‐catalyzed ortho C−H functionalization of N‐ nitrosoanilines with α ‐sulfonylcarbenes had been developed. The reaction was carried out under mild conditions and the products were obtained with good to excellent yields. The diverse transformations of the products to ortho ‐functionalized anilines and nitrogen heterocycles were achieved. Furthermore, a cascade reaction of N‐ nitrosoanilines and α ‐sulfonyl‐ α ‐diazo‐ketones provided 3‐sulfonyl‐indoles efficiently. magnified image

Topics & Concepts

ChemistrySulfonylSurface modificationDiazoCatalysisMedicinal chemistryNitrogenOrganic chemistryCombinatorial chemistryPhysical chemistryAlkylCatalytic C–H Functionalization MethodsCyclopropane Reaction MechanismsSynthesis and Catalytic Reactions
Rh(III)‐Catalyzed C−H Functionalization of <i>N‐</i>Nitrosoanilines with <i>α</i>‐Sulfonylcarbenes | Litcius