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Construction of the 2-Amino-1,3-selenazole Skeleton via PhICl<sub>2</sub>/KSeCN-Mediated Selenocyanation/Cyclization

Shanqing Tao, Lingzhi Xu, Kaiyue Yang, Jianing Zhang, Yunfei Du

2022Organic Letters34 citationsDOI

Abstract

/KSeCN-enabled electrophilic selenocyanation of β-enaminones and β-enamino esters followed by intramolecular cyclization under basic conditions. Compared to the classical Hantzsch strategy that utilizes selenourea or its analogues as starting materials or crucial intermediates, this method might represent an alternative approach for the assembly of 1,3-selenazole framework through a different pathway.

Topics & Concepts

ChemistrySkeleton (computer programming)Intramolecular forceElectrophileCombinatorial chemistryStereochemistryOrganic chemistryComputer scienceCatalysisProgramming languageOrganoselenium and organotellurium chemistrySulfur-Based Synthesis TechniquesOrganic and Inorganic Chemical Reactions
Construction of the 2-Amino-1,3-selenazole Skeleton via PhICl<sub>2</sub>/KSeCN-Mediated Selenocyanation/Cyclization | Litcius