Litcius/Paper detail

Palladacycle-Catalyzed Olefinic C–P Cross-Coupling of Alkenylsulfonium Salts with Diarylphosphines to Access Alkenylphosphines

Jie Zhu, Yun Ye, Yinhua Huang

2022Organometallics30 citationsDOI

Abstract

An efficient olefinic C–P cross-coupling of alkenylsulfonium salts with secondary diarylphosphines is reported. The use of a palladacycle enables the facile formation of a C–P bond at the alkenyl moiety of alkenylsulfonium salts tolerating a wide range of functional groups under mild conditions. This protocol provides an easy access to various alkenylphosphine products in good to high yields with high levels of stereoselectivity (E selectivity).

Topics & Concepts

ChemistryMoietyStereoselectivitySelectivityCatalysisCoupling (piping)Combinatorial chemistryStereochemistryMedicinal chemistryOrganic chemistryEngineeringMechanical engineeringSulfur-Based Synthesis TechniquesCatalytic C–H Functionalization MethodsAsymmetric Hydrogenation and Catalysis