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Preliminary Assessment of Tara Gum as a Wall Material: Physicochemical, Structural, Thermal, and Rheological Analyses of Different Drying Methods

Elibet Moscoso-Moscoso, Carlos A. Ligarda-Samanez, David Choque-Quispe, Mary L. Huamán-Carrión, José Carlos Arévalo Quijano, Germán De la Cruz, Rober Aníbal Luciano Alipio, Wilber César Calsina Ponce, Reynaldo Sucari León, Uriel Rigoberto Quispe Quezada, Dante Fermín Calderón Huamaní

2024Polymers16 citationsDOIOpen Access PDF

Abstract

seeds, was investigated in this study. Wall materials were produced using spray drying, forced convection, and vacuum oven drying. In addition, a commercial sample obtained through mechanical methods and direct milling was used as a reference. The gums exhibited low moisture content (8.63% to 12.55%), water activity (0.37 to 0.41), bulk density (0.43 to 0.76 g/mL), and hygroscopicity (10.51% to 11.42%). This allows adequate physical and microbiological stability during storage. Polydisperse particles were obtained, ranging in size from 3.46 µm to 139.60 µm. Fourier transform infrared spectroscopy characterisation confirmed the polysaccharide nature of tara gum, primarily composed of galactomannans. Among the drying methods, spray drying produced the gum with the best physicochemical characteristics, including higher lightness, moderate stability, smaller particle size, and high glass transition temperature (141.69 °C). Regarding rheological properties, it demonstrated a non-Newtonian pseudoplastic behaviour that the power law could accurately describe. The apparent viscosity of the aqueous dispersions of the gum decreased with increasing temperature. In summary, the results establish the potential of tara gum as a wall material applicable in the food and pharmaceutical industries.

Topics & Concepts

RheologyBiopolymerMaterials scienceGuar gumShear thinningSpray dryingLightnessApparent viscosityParticle sizeGlass transitionViscosityPolysaccharideComposite materialChemical engineeringChemistryPolymerChromatographyFood scienceOrganic chemistryPhysicsOpticsEngineeringPolysaccharides Composition and ApplicationsPolysaccharides and Plant Cell WallsProteins in Food Systems