Litcius/Paper detail

Quantitative analysis of dislocations in 4H-SiC wafers using synchrotron X-ray topography with ultra-high angular resolution

Hongyu Peng, Zeyu Chen, Yafei Liu, Balaji Raghothamachar, Xianrong Huang, Lahsen Assoufid, Michael Dudley

2022Journal of Applied Crystallography13 citationsDOIOpen Access PDF

Abstract

Utilization of an Si(331) beam conditioner together with an Si(111) double-crystal monochromator (DCM) enables the angular resolution of synchrotron X-ray topography to be increased by an order of magnitude compared with grazing-incidence topography or back-reflection topography conducted with the DCM alone. This improved technique with extremely small beam divergence is referred to as synchrotron X-ray plane-wave topography (SXPWT). This study demonstrates that the rocking curve width of 4H-SiC 0008 in PWT is only 2.5′′ and thus the lattice distortion at the scale of 1′′ will significantly affect the diffracted intensity. This work reports the ultra-high angular resolution in SXPWT which enables detailed probing of the lattice distortion outside the dislocation core in 4H-SiC, where the sign of the Burgers vector can be readily determined through comparison with ray-tracing simulations.

Topics & Concepts

SynchrotronMonochromatorOpticsBurgers vectorSynchrotron radiationDiffractionMaterials scienceX-rayPhysicsWavelengthTransmission electron microscopySilicon Carbide Semiconductor TechnologiesSilicon and Solar Cell TechnologiesThin-Film Transistor Technologies