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Cesium carbonate-catalyzed synthesis of phosphorothioates <i>via S</i>-phosphination of thioketones

Ze-Wei Chen, Pratheepkumar Annamalai, Rekha Bai, Yongyi Hu, Satpal Singh Badsara, Kuo‐Wei Huang, Chin‐Fa Lee

2022Chemical Communications16 citationsDOI

Abstract

A highly efficient and environmentally-friendly base-mediated transition metal-free direct thiophilic catalytic approach is reported for the synthesis of S -benzhydryl-phosphorothioates by reacting phosphite nucleophiles with diarylmethanethione.

Topics & Concepts

CaesiumCatalysisCarbonateChemistryCombinatorial chemistryInorganic chemistryOrganic chemistrySulfur-Based Synthesis TechniquesSynthesis and Reactivity of Sulfur-Containing CompoundsChemical Synthesis and Reactions
Cesium carbonate-catalyzed synthesis of phosphorothioates <i>via S</i>-phosphination of thioketones | Litcius