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Ni-Catalyzed Reductive Fluoroalkylacylation of Alkynes for the Steroselective Synthesis of Fluoroalkylated Enones

Zhuzhu Zhang, Jia-Jia Lei, Xiaohong Zhang, Xiaohong Zhang, Xing‐Guo Zhang, Xing‐Guo Zhang, Hai‐Yong Tu

2022Organic Letters16 citationsDOI

Abstract

A Ni-catalyzed three-component reductive fluoroalkylacylation of alkynes with fluoroalkyl halides and acyl chlorides is presented. This dicarbofunctionalization provides an efficient method for the synthesis of fluoroalkyl-incorporated enones under mild conditions with high yields and excellent regioselectivity and stereoselectivity.

Topics & Concepts

ChemistryRegioselectivityStereoselectivityCatalysisHalideCombinatorial chemistryMedicinal chemistryOrganic chemistryFluorine in Organic ChemistryCatalytic C–H Functionalization Methods
Ni-Catalyzed Reductive Fluoroalkylacylation of Alkynes for the Steroselective Synthesis of Fluoroalkylated Enones | Litcius