Litcius/Paper detail

Using Supercritical Fluid Technologies to Prepare Micro- and Nanoparticles

A. M. Vorobei, О. О. Паренаго

2021Russian Journal of Physical Chemistry A30 citationsDOI

Abstract

Abstract Literature data on basic research for and practical application of the synthesis of micro- and nanoparticles with the use of supercritical fluids (SCFs) are systematized and analyzed. The review of SCF-based micronization is divided into sections according to the role played by an SCF in the process, which is in most cases a solvent (the rapid expansion of supercritical solutions (RESS)), an antisolvent (supercritical antisolvent precipitation (SAS)), or a solute (particles formed from gas-saturated solutions (PGSS)). Special attention is given to means less covered in the literature, where the SCF is a co-solute (SAA, CAN-BD, and DELOS). The main advantages, limitations, and applicability of each approach for a specific range of substances are analyzed in detail. It is shown that the range of the considered substances is not limited to the best-described pharmaceutical objects; rather, it is greatly expanded to cover possible applications of SCF micronization. The focus is mainly on works published over the last decade.

Topics & Concepts

MicronizationSupercritical fluidNanoparticlePrecipitationSolventNanotechnologyMaterials scienceChemistryChemical engineeringParticle sizeOrganic chemistryEngineeringPhysicsPhysical chemistryMeteorologyPhase Equilibria and ThermodynamicsAnalytical Chemistry and ChromatographySubcritical and Supercritical Water Processes