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Visible-light promoted α-alkylation of glycine derivatives with alkyl boronic acids

Jiayuan Wang, Yingpeng Su, Zheng‐Jun Quan, Jun Li, Jie Yang, Yong Yuan, Congde Huo

2021Chemical Communications48 citationsDOI

Abstract

A visible-light-mediated aerobic α-alkylation reaction of glycine derivatives with alkyl boronic acids has been established in the presence of a Ru/Cu catalyst system, giving the desired radical coupling products efficiently. The transformation features mild reaction conditions and broad substrate scope, delivering a wide range of complex unnatural α-amino-acid derivatives.

Topics & Concepts

AlkylationAlkylGlycineChemistryBoronic acidCombinatorial chemistryOrganic chemistryAmino acidCatalysisBiochemistryRadical Photochemical ReactionsCatalytic C–H Functionalization MethodsOxidative Organic Chemistry Reactions
Visible-light promoted α-alkylation of glycine derivatives with alkyl boronic acids | Litcius