Litcius/Paper detail

Initiation-Confined Holographic Photopolymerization under Visible Light

Jie Chen, Wei Wei, Haiyan Peng, Mingli Ni, Hongxi Guo, Dengfu Lu, Yonggui Liao, Xingping Zhou, Zhong’an Li, Xiaolin Xie

2025Journal of the American Chemical Society9 citationsDOI

Abstract

Holographic photopolymerization provides a robust approach for the advanced manufacturing of structurally ordered devices. However, photogenerated radicals in bright regions are prone to cross-regional diffusion and induce unwanted polymerizations in dark regions, making efficient holographic manufacturing exceedingly challenging. Herein, we report a breakthrough by spatially confining the initiation function, enabling the unprecedentedly rapid formation of predesigned submicron-ordered grating structures within merely 0.75 s under visible light holographic exposure. Theoretical computations attribute the success of this initiation-confined approach to orders of magnitude larger reaction rate constants of initiation than propagation. This approach is highly versatile, facilitating the fabrication of both transmission- and reflection-type volume holographic grating structures starting from various reaction systems, and the refractive index modulation can be as high as 0.10, enabling ultraefficient manufacturing of waveguide combiners for high-fidelity near-eye AR displays.

Topics & Concepts

HolographyPhotopolymerGratingChemistryRefractive indexOpticsOptoelectronicsDiffusionPolymerMaterials sciencePolymerizationPhysicsOrganic chemistryThermodynamicsAdvanced Optical Imaging TechnologiesPhotopolymerization techniques and applicationsPhotorefractive and Nonlinear Optics