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Ppb-Level Photoacoustic Detection of Chloroform Using Four-Microphone Array

Dou Dou, Mingqi Jiao, Mingyang Feng, Mu Liang, Kaijun Mu, Yingying Qiao, Lei Li, Chongxin Shan

2025Analytical Chemistry13 citationsDOI

Abstract

The photoacoustic spectroscopy (PAS) system commonly enhances the efficiency of optical-acoustic-electrical energy conversion by increasing the laser power, optimizing the resonance characteristics of the photoacoustic cell (PAC), and improving the sensitivity of acoustic sensors. However, conventional systems using a single-microphone or a dual-microphone differential setup for point sampling of the photoacoustic signal fail to account for its spatial distribution, leading to a loss of spatial gain. Drawing on microphone array theory derived from sonar technology, this study, for the first time, presents a PAS sensing system based on a four-microphone array, which is applied to detect chloroform gas. The microphones are positioned at 90° intervals around the PAC resonance chamber wall, enhancing the spatial sampling rate of the signals. A digital phase-locked algorithm demodulates the combined signals from the four microphones into the concentration data. Experimental results show that, compared to a single-microphone system, the four-microphone array system increases sensitivity by a factor of 4, doubles the signal-to-noise ratio, and achieves a minimum detection limit of 69 ppb, demonstrating a significant improvement in sensitivity by capturing the spatial distribution of PA signals.

Topics & Concepts

MicrophoneSensitivity (control systems)AcousticsSIGNAL (programming language)Sampling (signal processing)Photoacoustic imaging in biomedicineMicrophone arrayNoise (video)Photoacoustic spectroscopyPhotoacoustic effectSignal-to-noise ratio (imaging)ChemistryOpticsPhysicsComputer scienceElectronic engineeringEngineeringSound pressureProgramming languageDetectorImage (mathematics)Artificial intelligenceSpectroscopy and Laser ApplicationsPhotoacoustic and Ultrasonic ImagingAdvanced Chemical Sensor Technologies
Ppb-Level Photoacoustic Detection of Chloroform Using Four-Microphone Array | Litcius