Litcius/Paper detail

Nickel-Catalyzed Decarbonylative Reductive Alkylation of Aroyl Fluorides with Alkyl Bromides

Qiang Chen, Jingwen You, Tian Tian, Zhenyao Li, Myuto Kashihara, Hiroki Mori, Yasushi Nishihara

2022Organic Letters18 citationsDOI

Abstract

This paper describes the nickel-catalyzed reductive alkylation of aroyl fluorides with alkyl bromides in a decarbonylative manner. In this reaction, various functional groups are well tolerated and the C(sp2)–C(sp3) bond can be constructed directly without the use of organometallic reagents. The present reaction is a cross-electrophile coupling via the radical pathway, affording the corresponding alkylarenes in moderate to good yields.

Topics & Concepts

ChemistryAlkylationAlkylReagentCatalysisElectrophileNickelReductive eliminationMedicinal chemistryCombinatorial chemistryOrganic chemistryCatalytic C–H Functionalization MethodsFluorine in Organic ChemistryRadical Photochemical Reactions
Nickel-Catalyzed Decarbonylative Reductive Alkylation of Aroyl Fluorides with Alkyl Bromides | Litcius