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Austenite Reversion Behavior of Maraging Steel Additive-manufactured by Laser Powder Bed Fusion

Naoki Takata, Yuya Ito, Ryoya Nishida, Asuka Suzuki, Makoto Kobashi, Masaki Kato

2023ISIJ International11 citationsDOIOpen Access PDF

Abstract

This study was set to fundamentally investigate the characteristics of austenite reversion occurring in maraging steels additive-manufactured by laser powder bed fusion (L-PBF). The maraging steel samples manufactured under different L-PBF process conditions (laser power P and scan speed v) were subjected to heat treatments at 550 oC for various durations, compared with the results of the austenitized and water-quenched sample with fully martensite structure. The L-PBF manufactured samples exhibited the martensite structure (including localized austenite (γ) phases) containing submicron-sized cellular structures. Enriched alloy elements were detected along the cell boundaries, whereas such cellar structure was not found in the water-quenched sample. The localized alloy elements can be rationalized by the continuous variations in the γ-phase composition in solidification during the L-PBF process. The precipitation of nanoscale intermetallic phases and the following austenitic reversion occurred in all of the experimental samples. The L-PBF manufactured samples exhibited faster kinetics of the precipitation and austenite reversion than the water-quenched sample at elevated temperatures. The kinetics changed depending on the L-PBF process condition. The enriched Ni element (for stabilizing γ phase) localized at cell boundaries would play a role in the nucleation site for the formation of γ phase at 550 oC, resulting in enhanced austenite reversion in the L-PBF manufactured samples. The variation in the reaction kinetics depending on the L-PBF condition would be due to the varied thermal profiles of the manufactured samples by consecutive scanning laser irradiation operated under different P and v values.

Topics & Concepts

AusteniteMaterials scienceMaraging steelMartensiteMetallurgyAlloyPrecipitationIntermetallicKineticsOrthorhombic crystal systemNucleationPhase (matter)MicrostructureCrystallographyThermodynamicsCrystal structureChemistryOrganic chemistryPhysicsMeteorologyQuantum mechanicsAdditive Manufacturing Materials and ProcessesWelding Techniques and Residual StressesAdditive Manufacturing and 3D Printing Technologies
Austenite Reversion Behavior of Maraging Steel Additive-manufactured by Laser Powder Bed Fusion | Litcius