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Different Lewis Acid Promotor-Steered Highly Regioselective Phosphorylation of Tertiary Enamides

Wenzhong Li, Ran Shi, Xuesi Zhang, Sen Chen, Yu Wang, Mengqi Wang, Bin Yang, Jiazhu Li, Xin‐Ming Xu

2022The Journal of Organic Chemistry21 citationsDOI

Abstract

Different Lewis acid promotor-steered highly regioselective phosphorylation of tertiary enamides with diverse H-phosphonates or H-phosphine oxides was developed. Under the catalysis of iron salt, the phosphonyl group was introduced into the α-position of tertiary enamides, affording various α-phosphorylated amides in high efficiency. On the other hand, the β-phosphorylated tertiary enamides were efficiently obtained as the products in the presence of manganese(III) acetylacetonate.

Topics & Concepts

RegioselectivityChemistryPhosphinePhosphorylationLewis acids and basesManganeseCatalysisPromoterCombinatorial chemistryOrganic chemistryBiochemistryGeneGene expressionOrganophosphorus compounds synthesisChemical Synthesis and AnalysisAsymmetric Hydrogenation and Catalysis
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