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Anthraquinone Redox Relay for Dye‐Sensitized Photo‐electrochemical H<sub>2</sub>O<sub>2</sub> Production

Jiaonan Sun, Yiying Wu

2020Angewandte Chemie International Edition52 citationsDOIOpen Access PDF

Abstract

Abstract Anthraquinone (AQ) redox mediators are introduced to metal‐free organic dye sensitized photo‐electrochemical cells (DSPECs) for the generation of H 2 O 2 . Instead of directly reducing O 2 to produce H 2 O 2 , visible‐light‐driven AQ reduction occurs in the DSPEC and the following autooxidation with O 2 allows H 2 O 2 accumulation and AQ regeneration. In an aqueous electrolyte, under 1 sun conditions, a water‐soluble AQ salt is employed with the highest photocurrent of up to 0.4 mA cm −2 and near‐quantitative faradaic efficiency for producing H 2 O 2 . In a non‐aqueous electrolyte, under 1 sun illumination, an organic‐soluble AQ is applied and the photocurrent reaches 1.8 mA cm −2 with faradaic efficiency up to 95 % for H 2 O 2 production. This AQ‐relay DSPEC exhibits the highest photocurrent so far in non‐aqueous electrolytes for H 2 O 2 production and excellent acid stability in aqueous electrolytes, thus providing a practical and efficient strategy for visible‐light‐driven H 2 O 2 production.

Topics & Concepts

PhotocurrentRedoxAqueous solutionFaraday efficiencyElectrolyteAnthraquinoneElectrochemistryChemistryOxygen evolutionInorganic chemistryPhotochemistryMaterials scienceElectrodeOrganic chemistryPhysical chemistryOptoelectronicsAdvanced Photocatalysis TechniquesPerovskite Materials and ApplicationsTiO2 Photocatalysis and Solar Cells
Anthraquinone Redox Relay for Dye‐Sensitized Photo‐electrochemical H<sub>2</sub>O<sub>2</sub> Production | Litcius