Litcius/Paper detail

Thermal and optical properties of PMMA films reinforced with Nb2O5 nanoparticles

Barbara Hajduk, Henryk Bednarski, Paweł Jarka, Henryk Janeczek, Marcin Godzierz, Tomasz Tański

2021Scientific Reports49 citationsDOIOpen Access PDF

Abstract

Abstract The article presents the thermal and physical properties of PMMA composite films with the addition of Nb 2 O 5 nanoparticles. The addition of nanoparticles to PMMA mainly influenced the optical transmission and glass transition temperature of composite films compared to pure PMMA. It is clearly visible in the results of the conducted ellipsometric and differential scanning calorimetry tests. X-ray studies showed that the heat treatment of the samples resulted in the ordering of the polymer structure (flattening of the polymer chains). Examining the surface of the samples with scanning electron microscopy, it can be seen that Nb 2 O 5 nanoparticles formed unusual, branched formations resembling "snowflakes".

Topics & Concepts

Differential scanning calorimetryNanoparticleMaterials sciencePolymerGlass transitionComposite numberScanning electron microscopeTransmission electron microscopyComposite materialChemical engineeringOptical microscopeThermalNanotechnologyPhysicsEngineeringMeteorologyThermodynamicsMaterial Properties and ApplicationsPolymer Nanocomposite Synthesis and IrradiationThermal and Kinetic Analysis