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Mechanical and thermal properties of δ‐RE <sub>4</sub> Hf <sub>3</sub> O <sub>12</sub> (RE = Yb, Lu)

Wanpeng Hu, Guangheng Zhang, Yiming Lei, Luchao Sun, Jie Zhang, Jingyang Wang

2022International Journal of Applied Ceramic Technology21 citationsDOI

Abstract

Abstract Rare‐earth (RE) hafnates are promising thermal and environmental barrier coating (TEBC) materials for SiC f /SiC ceramic matrix composites. In this study, pure‐phase and dense δ‐RE 4 Hf 3 O 12 (RE = Yb, Lu) bulk ceramics have been fabricated via a hot‐pressing method. The crystal structure, microstructure, mechanical, and thermal properties of δ‐RE 4 Hf 3 O 12 were systematically investigated in order to probe their potential application as TEBCs. The high‐temperature elastic moduli of δ‐Yb 4 Hf 3 O 12 and δ‐Lu 4 Hf 3 O 12 are measured to be 185 and 188 GPa at 1673 K, respectively, which are over 85% values of room temperature. The coefficients of thermal expansion are 7.64 × 10 −6 and 7.46 × 10 −6 K −1 for δ‐Yb 4 Hf 3 O 12 and δ‐Lu 4 Hf 3 O 12 , respectively. The relatively low coefficient of thermal expansion and thermal conductivity as well as their excellent high‐temperature stability endow these hafnates as potential TEBC candidates.

Topics & Concepts

Materials scienceThermal expansionCeramicThermal conductivityMicrostructureThermal stabilityThermal barrier coatingHot pressingPhase (matter)Ceramic matrix compositeAnalytical Chemistry (journal)Composite materialChemical engineeringOrganic chemistryChromatographyChemistryEngineeringAdvanced ceramic materials synthesisAdvanced materials and compositesNuclear materials and radiation effects
Mechanical and thermal properties of δ‐RE <sub>4</sub> Hf <sub>3</sub> O <sub>12</sub> (RE = Yb, Lu) | Litcius