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Nickel-Catalyzed Deaminative Ketone Synthesis: Coupling of Alkylpyridinium Salts with Thiopyridine Esters via C–N Bond Activation

I. N. Chaithanya Kiran, Ramagonolla Kranthikumar

2023Organic Letters14 citationsDOI

Abstract

A direct synthesis of ketones by the nickel-catalyzed deaminative cross-coupling of alkylpyridinium salts with thiopyridine esters has been reported. The reaction works well for both primary and secondary amines. This approach affords a highly valuable vista for the facile synthesis of ketones from easily accessible feedstock chemicals. The utility of this method is demonstrated through the functionalization of complex bioactives and pharmaceuticals.

Topics & Concepts

ChemistryCatalysisKetoneNickelPrimary (astronomy)Organic chemistrySurface modificationCombinatorial chemistryCoupling reactionPhysical chemistryAstronomyPhysicsCatalytic C–H Functionalization MethodsSulfur-Based Synthesis TechniquesCatalytic Cross-Coupling Reactions
Nickel-Catalyzed Deaminative Ketone Synthesis: Coupling of Alkylpyridinium Salts with Thiopyridine Esters via C–N Bond Activation | Litcius