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Combined photoredox/engineered P450 enzymatic direct dioxygen-functionalization of arylalkanes to chiral acyloins

Jing Wang, Hezhen Wang, Chunyong Wei, Lei Zhang, Bao‐Dong Cui, Zhongqiang Wang, Yun Zhang, Nan‐Wei Wan, Haji Akber Aisa, Yong‐Zheng Chen

2022Organic & Biomolecular Chemistry16 citationsDOI

Abstract

was developed by the direct carbonylation of aromatic methyl C-H bonds and subsequently combined with the aerobic P450-biocatalytic enantioselective hydroxylation of intermediate ketones, thus providing a green and sustainable approach towards optically pure acyloins.

Topics & Concepts

ChemistryHydroxylationPhotoredox catalysisCombinatorial chemistrySurface modificationEnantioselective synthesisCatalysisBiocatalysisOrganocatalysisRedoxCarbonylationOrganic chemistryEnzymePhotocatalysisReaction mechanismPhysical chemistryCarbon monoxideCatalytic C–H Functionalization MethodsRadical Photochemical ReactionsSulfur-Based Synthesis Techniques
Combined photoredox/engineered P450 enzymatic direct dioxygen-functionalization of arylalkanes to chiral acyloins | Litcius