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Tribological properties of hydroxyapatite-coated nanorods on Ti-6Al-4V surfaces

Sarah Akua Osafo, Tabiri Kwayie Asumadu, Desmond Klenam, Precious Osayamen Etinosa, John D. Obayemi, Benjamin Agyei‐Tuffour, Abu Yaya, David Dodoo‐Arhin, S. C. Eluu, W. O. Soboyejo

2025Scientific Reports11 citationsDOIOpen Access PDF

Abstract

This paper presents the tribological properties and bioactivity of nanostructured hydroxyapatite (HA) from biowaste sources and coated onto Ti-6Al-4V substrates using a novel pack cementation method. The process introduced HA pillars/nanorods on the surfaces of Ti-6Al-4V to enhance their osseointegration for dental implants. The mechanical and tribological properties were studied with nanoindentation, and pin-on-disk techniques, following the microstructural characterization of the coatings with atomic force microscopy, X-ray diffraction, Raman spectroscopy, scanning electron microscopy, and energy dispersive x-ray spectroscopy. The study also examines the surface bioactivity and elucidates the underlying friction and wear mechanisms of the HA-coated and annealed Ti-6Al-4V surface. The study results show a bone bonding capacity of the biowaste-derived HA-coated substrate with improved hardness and tribological properties. The implications of the study are discussed for the development of nano-structured HA-coated Ti-6Al-4V for dental implants with improved osseointegration for dental and biomedical applications.

Topics & Concepts

NanoindentationMaterials scienceTribologyOsseointegrationScanning electron microscopeNanorodRaman spectroscopyCementation (geology)Composite materialNanotechnologyCementImplantPhysicsSurgeryMedicineOpticsBone Tissue Engineering MaterialsOrthopaedic implants and arthroplastyTitanium Alloys Microstructure and Properties
Tribological properties of hydroxyapatite-coated nanorods on Ti-6Al-4V surfaces | Litcius