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Stable 1T‐MoS<sub>2</sub> by Facile Phase Transition Synthesis for Efficient Electrocatalytic Oxygen Evolution Reaction

Ranjith Kumar Dharman, Hyeonae Im, Mrinal Kanti Kabiraz, Jeonghyeon Kim, Kiran P. Shejale, Sang‐Il Choi, Jeong Woo Han, Sung Yeol Kim

2024Small Methods35 citationsDOI

Abstract

Abstract The 1T phase of MoS 2 exhibits much higher electrocatalytic activity and better stability than the 2H phase. However, the harsh conditions of 1T phase synthesis remain a significant challenge for various extensions and applications of MoS 2 . In this work, a simple hydrothermal‐based synthesis method for the phase transition of MoS 2 is being developed. For this, the NH 2 ‐MIL‐125(Ti) (Ti MOF) is successfully utilized to induce the phase transition of MoS 2 from 2H to 1T, achieving a high conversion ratio of ≈78.3%. The optimum phase‐induced MoS 2 /Ti MOF heterostructure demonstrates enhanced oxygen evolution reaction (OER) performance, showing an overpotential of 290 mV at a current density of 10 mA cm −2 . The density functional theory (DFT) calculations are demonstrating the benefits of this phase transition, determining the electronic properties and OER performance of MoS 2 .

Topics & Concepts

OverpotentialOxygen evolutionMaterials scienceDensity functional theoryPhase (matter)Phase transitionHydrothermal circulationTransition metalHeterojunctionChemical engineeringCatalysisOxygenNanotechnologyPhysical chemistryOptoelectronicsChemistryComputational chemistryThermodynamicsElectrochemistryElectrodePhysicsOrganic chemistryEngineeringElectrocatalysts for Energy ConversionFuel Cells and Related MaterialsAdvanced Photocatalysis Techniques
Stable 1T‐MoS<sub>2</sub> by Facile Phase Transition Synthesis for Efficient Electrocatalytic Oxygen Evolution Reaction | Litcius