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Luminescent Fe(III) Complex Sensitizes Aerobic Photon Upconversion and Initiates Photocatalytic Radical Polymerization

Pengyue Jin, Xinhuan Xu, Yongli Yan, Heinrich Hammecke, Cui Wang

2024Journal of the American Chemical Society34 citationsDOIOpen Access PDF

Abstract

with 9,10-diphenylanthracene (DPA) as the annihilator achieves a 6-fold enhancement to ∼0.2% in aerated solution at room temperature. The singlet excited state of DPA, accessed via photon upconversion in the Fe(III)/DPA pair, allows efficient photoredox catalytic radical polymerization of acrylate monomers in a spatially controlled manner, whereas this process is kinetically hindered with the prompt DPA. Our study provides a new strategy of using low-cost iron and low-energy visible light for efficient polymer synthesis, which is a significant step for both fundamental research and future applications.

Topics & Concepts

ChemistryPhotochemistryPhoton upconversionIridiumExcited stateRutheniumPhotosensitizerAnthraceneIntersystem crossingTriplet statePhotocatalysisEnergy transformationCatalysisMoleculeSinglet stateOrganic chemistryPhysicsThermodynamicsNuclear physicsIonLuminescence and Fluorescent MaterialsNanoplatforms for cancer theranosticsRadical Photochemical Reactions