Litcius/Paper detail

An electrochemical cascade process: synthesis of 3-selenylindoles from 2-alkynylanilines with diselenides

Anil Balajirao Dapkekar, Gedu Satyanarayana

2023Chemical Communications43 citationsDOI

Abstract

Substituted organoselenium compounds are crucial structural motifs in pharmaceutical molecules. Herein, we report a metal, oxidant, and base-free electrochemical approach to access 3-selenylindoles through an oxidative cyclization of 2-alkynylanilines with diselenides. This environmentally friendly approach demonstrates a wide range of substrate scope under mild reaction conditions in an electrochemical undivided cell setup.

Topics & Concepts

ElectrochemistryCombinatorial chemistryEnvironmentally friendlyCascadeSubstrate (aquarium)Scope (computer science)Base (topology)MoleculeChemistryProcess (computing)NanotechnologyMaterials scienceOrganic chemistryComputer scienceMathematicsBiologyOperating systemEcologyMathematical analysisPhysical chemistryElectrodeProgramming languageGeologyChromatographyOceanographySulfur-Based Synthesis TechniquesRadical Photochemical ReactionsCatalytic C–H Functionalization Methods