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Multiple Accessible Redox-Active Sites in a Robust Covalent Organic Framework for High-Performance Potassium Storage

Xueling Chen, Mo Xie, Ze‐Lin Zheng, Xiao Luo, Hongchang Jin, Yanfei Chen, Guo‐Zhan Yang, De‐Shan Bin, Dan Li

2023Journal of the American Chemical Society178 citationsDOI

Abstract

Covalent organic framework (COF) materials with porous character and robust structure have significant applied implications for K-ion battery (KIB) anodes, but they are limited by the low reversible capacity and inferior rate capability. Here, based on theoretical calculations, we identified that a porous bulk COF featuring numerous pyrazines and carbonyls in the π-conjugated periodic skeleton could provide multiple accessible redox-active sites for high-performance potassium storage. Its porous structure with a surface-dominated storage mechanism enabled the fast and stable storage of K-ions. Its insolubility in organic electrolytes and small volumetric change after potassiation ensured a robust electrode for stable cycling. As a KIB anode, this bulk COF demonstrated an unprecedentedly outstanding combination of reversible capacity (423 mAh g –1 at 0.1 C), rate capability (185 mAh g –1 at 10 C), and cyclability. The theoretical simulation and comprehensive characterizations confirmed the active sites are contributed by C═O, C═N, and the cation−π effect.

Topics & Concepts

ChemistryAnodeRedoxElectrolyteCovalent bondPorosityPotassiumCovalent organic frameworkIonConjugated systemChemical engineeringElectrodeInorganic chemistryOrganic chemistryPhysical chemistryPolymerEngineeringAdvanced battery technologies researchAdvanced Battery Materials and TechnologiesCovalent Organic Framework Applications