Combined, time-resolved, <i>in situ</i> neutron reflectometry and X-ray diffraction analysis of dynamic SEI formation during electrochemical N<sub>2</sub> reduction
Sarah J. Blair, Mathieu Doucet, Valerie A. Niemann, Kevin H. Stone, Melissa E. Kreider, James F. Browning, Candice E. Halbert, Hanyu Wang, Peter Benedek, Eric J. McShane, Adam C. Nielander, Alessandro Gallo, Thomas F. Jaramillo
Abstract
In situ neutron reflectometry and GI-XRD reveal the dynamics of SEI formation and layer composition during Li-NRR with current cycling.
Topics & Concepts
Neutron reflectometryReflectometryX-rayElectrochemistryNeutron diffractionIn situMaterials scienceDiffractionX-ray crystallographyReduction (mathematics)Analytical Chemistry (journal)NeutronChemistryCrystallographyPhysicsOpticsNuclear physicsElectrodeNeutron scatteringPhysical chemistryTime domainComputer scienceChromatographyMathematicsSmall-angle neutron scatteringGeometryComputer visionOrganic chemistryAmmonia Synthesis and Nitrogen ReductionHydrogen Storage and MaterialsInorganic Chemistry and Materials