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The Hard X-ray Nanoprobe beamline at Diamond Light Source

Paul D. Quinn, Lucia Alianelli, Miguel A. Gomez‐Gonzalez, David A. Mahoney, Fernando Cacho‐Nerin, Andrew Peach, Julia E. Parker

2021Journal of Synchrotron Radiation66 citationsDOIOpen Access PDF

Abstract

The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differential phase contrast and ptychography. The 185 m-long beamline operates over a 5 keV to 23 keV energy range providing a ≤50 nm beam size for routine user experiments and a flexible scanning system allowing fast acquisition. The beamline achieves robust and stable operation by imaging the source in the vertical direction and implementing horizontally deflecting primary optics and an overfilled secondary source in the horizontal direction. This paper describes the design considerations, optical layout, aspects of the hardware engineering and scanning system in operation as well as some examples illustrating the beamline performance.

Topics & Concepts

BeamlineOpticsDiamondSynchrotronNanoprobeMaterials scienceBeam (structure)PhysicsFluorescenceComposite materialAdvanced X-ray Imaging TechniquesAdvanced X-ray and CT ImagingAdvanced Electron Microscopy Techniques and Applications
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