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A panoramic view on synthetic applications of α-oxothioamides: a highly regioselective synthesis of 2-acyl-4-(het)arylthiazoles and thioethers

Rajaghatta N. Suresh, Toreshettahally R. Swaroop, Darshini Gowda, Kempegowda Mantelingu, Kanchugarakoppal S. Rangappa

2023RSC Advances31 citationsDOIOpen Access PDF

Abstract

Highly regioselective synthesis of 2-acyl-4-(het)arylthiazoles and thioethers by the reaction between α-oxothioamides and α-bromoketones in the absence of base in DMF and in the presence of triethylamine in acetonitrile, respectively, has been reported. This thiazole synthesis is an important extended work of the Hantzsch thiazole synthesis, which overcomes the drawbacks of earlier reported methods. The probable mechanisms for the formation of thiazoles and thioethers are also presented.

Topics & Concepts

RegioselectivityChemistryCombinatorial chemistryComputer scienceOrganic chemistryCatalysisSulfur-Based Synthesis TechniquesSynthesis and Reactivity of Sulfur-Containing CompoundsSynthesis of heterocyclic compounds