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Synthesis, spectroscopic properties, structural characterization, and computational studies of a new non-centrosymmetric hybrid compound: bis-cyanato-<i>N</i> chromium(<scp>iii</scp>) <i>meso</i>-arylporphyrin complex

Mondher Dhifet, Nabil Benzerroug, Tahani Mazyad Almutairi, Khadra B. Alomari, Nikolay Tumanov, Noureddine Issaoui

2025RSC Advances5 citationsDOIOpen Access PDF

Abstract

-N (axial ligand) distances from the bis-cyanate ligand are 2.012(3) Å and 2.016(4) Å. Crystal packing cohesion was stabilized by unconventional intramolecular C-H⋯O and C-H⋯Cl hydrogen bonds. In addition, we conducted a theoretical investigation of several key physical properties to provide a comprehensive understanding of the electron charge transfer mechanisms of the chromium(iii) porphyrin complex using density functional theory (DFT) at the B3LYP-D3/LanL2DZ level. This includes the analysis of frontier molecular orbitals (FMOs) and associated reactivity descriptors; molecular electrostatic potential (MEP) assessment; non-covalent interaction (NCI) analysis through reduced density gradient (RDG) surfaces and bond critical points (BCPs); as well as electron localization function (ELF), localized orbital locator (LOL), and Hirshfeld surface analyses.

Topics & Concepts

ChemistryIntramolecular forceTriclinic crystal systemDensity functional theoryMolecular orbitalCrystallographyElectron densityHydrogen bondAtomic orbitalChemical physicsPorphyrinElectron localization functionCrystal (programming language)Crystal structureReactivity (psychology)Computational chemistryCharge densitySingle crystalMoleculeIonic bondingLigand (biochemistry)Bond lengthElectron transferElectron diffractionTautomerIonMolecular geometryElectrostaticsElectronSynthesis and Characterization of Heterocyclic CompoundsSynthesis and biological activitySynthesis and Reactivity of Sulfur-Containing Compounds
Synthesis, spectroscopic properties, structural characterization, and computational studies of a new non-centrosymmetric hybrid compound: bis-cyanato-<i>N</i> chromium(<scp>iii</scp>) <i>meso</i>-arylporphyrin complex | Litcius