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Direct <i>in situ</i> spectroscopic evidence of the crucial role played by surface oxygen vacancies in the O<sub>2</sub>-sensing mechanism of SnO<sub>2</sub>

Stefan Kucharski, Pilar Ferrer, Federica Venturini, Georg Held, Alex S. Walton, Conor Byrne, James A. Covington, Sai Kiran Ayyala, Andrew M. Beale, Christopher S. Blackman

2022Chemical Science49 citationsDOIOpen Access PDF

Abstract

NAP-XPS characterisation of SnO 2 under operando conditions shows that resistance change, band bending and surface O-vacancy concentration are correlated with ambient O 2 concentration, challenging current preconceptions of gas sensor function.

Topics & Concepts

OxygenX-ray photoelectron spectroscopyStoichiometryGas phaseChemical physicsChemistrySynchrotron radiationAnalytical Chemistry (journal)Materials scienceChemical engineeringPhysical chemistryEnvironmental chemistryOpticsEngineeringPhysicsOrganic chemistryGas Sensing Nanomaterials and SensorsAnalytical Chemistry and SensorsZnO doping and properties
Direct <i>in situ</i> spectroscopic evidence of the crucial role played by surface oxygen vacancies in the O<sub>2</sub>-sensing mechanism of SnO<sub>2</sub> | Litcius