Litcius/Paper detail

Benzannulation with Et<sub>3</sub>N as 1,3-Diene Variants

Lipeng Long, Wenjia Wang, Yuping Zhu, Wenjun Luo, Yi Zhang, Juxiu Chen, Yuting Wei, Zhengwang Chen

2023Organic Letters12 citationsDOI

Abstract

With triethylamine as a 1,3-diene variant, a simple and practical process for the synthesis of phthalimides has been developed from readily available maleimide. The transformation can be performed in the absence of a metal catalyst with high levels of functional group tolerance. Various phthalimide compounds were constructed in moderate to good yields under mild conditions. Mechanism research indicates that oxygen and acid also play crucial roles in this reaction.

Topics & Concepts

PhthalimidesChemistryDienePhthalimideTriethylamineCatalysisMaleimideFunctional groupCombinatorial chemistryOrganic chemistryPolymerNatural rubberCatalytic C–H Functionalization MethodsSynthesis and Catalytic ReactionsClick Chemistry and Applications