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Refinement of the grain structure of additive manufactured titanium alloys via epitaxial recrystallization enabled by rapid heat treatment

Zhiyi Zou, Marco Simonelli, Juliano Katrib, Georgios Dimitrakis, Richard Hague

2020Scripta Materialia131 citationsDOIOpen Access PDF

Abstract

The coarse prior-β grain structure in titanium alloys produced by additive manufacturing is associated to mechanical anisotropy and limited fatigue life. Here we report a novel methodology to refine such structure by rapid heat treatment of Ti–6Al–4V produced by laser powder-bed fusion. The refinement was analysed using high-temperature EBSD that showed, for the first time, how high angle boundary β grains nucleated and grew with quasi-equiaxed morphology by epitaxial recrystallization. These findings show the potential for such heating regime to be applied to control grain size, morphology and distribution in a wider category of structural alloys produced by additive manufacturing.

Topics & Concepts

Materials scienceEquiaxed crystalsRecrystallization (geology)Electron backscatter diffractionTitanium alloyFusionMetallurgyTitaniumGrain boundaryMicrostructureAlloyPaleontologyLinguisticsBiologyPhilosophyAdditive Manufacturing Materials and ProcessesTitanium Alloys Microstructure and PropertiesHigh Entropy Alloys Studies
Refinement of the grain structure of additive manufactured titanium alloys via epitaxial recrystallization enabled by rapid heat treatment | Litcius