Litcius/Paper detail

Insight Notes: Considerations in the XPS Analysis of O1s Spectra for Metal Oxides

Alexander Graf, Mark A. Isaacs, David Morgan

2025Surface and Interface Analysis38 citationsDOIOpen Access PDF

Abstract

ABSTRACT The oxygen, O1s core level, is diagnostic in the study of metal oxides, revealing the formation of hydroxides, carbonates and other oxygen‐containing species in X‐ray photoelectron spectroscopy (XPS). This insight paper gives an overview of the complexities that may be overlooked in the analysis of oxygen core‐level spectra and aims to give practitioners of the technique a reasoned approach to the assignment of oxygen speciation.

Topics & Concepts

X-ray photoelectron spectroscopySpectral lineMetalOxygenMaterials scienceCore (optical fiber)SpectroscopyChemistryAnalytical Chemistry (journal)Transition metalElectron spectroscopyChemical physicsPhysical chemistryInorganic chemistryNanotechnologyElectron and X-Ray Spectroscopy TechniquesAdvanced Electron Microscopy Techniques and ApplicationsX-ray Spectroscopy and Fluorescence Analysis