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High Performance H<sub>2</sub>S Sensor Based on Ordered Fe<sub>2</sub>O<sub>3</sub>/Ti<sub>3</sub>C<sub>2</sub> Nanostructure at Room Temperature

Changkun Qiu, Hao Zhang, Qingrun Li, Yifan Song, Fei An, Haozhi Wang, Shiqiang Wang, Liang Zhu, Dongzhi Zhang, Zhe Yang

2024ACS Sensors22 citationsDOI

Abstract

The utilization of a heterogeneous nanojunction design has shown significant enhancements in the gas sensing capabilities of traditional metal oxide gas sensors. In this study, a novel room temperature H 2 S gas sensor employing Fe 2 O 3 functionalized Ti 3 C 2 MXene as the sensing material has been developed. This sensor exhibits a broad detection range (0.01–500 ppm), low detection limit (10 ppb), and rapid response/recovery times (10 s/15 s), making it ideal for ppb-level H 2 S detection. The exceptional gas sensitivity of Fe 2 O 3 /Ti 3 C 2 composite to H 2 S can be attributed to several key factors. First, the unique layered frame structure of Fe 2 O 3 /Ti 3 C 2 significantly amplifies the surface area of the hybrid material, enhancing the absorption and diffusion capabilities of H 2 S molecules. Second, the abundance of functional groups (–O, –OH, and –F) on the surface of Ti 3 C 2 MXene nanosheets provides additional active sites for H 2 S adsorption, The density functional theory calculation confirms that the adsorption energy of the Fe 2 O 3 /Ti 3 C 2 composite for H 2 S (−2.93 eV) is significantly lower than that of pure Fe 2 O 3 (−2.37 eV) and Ti 3 C 2 (−0.2 eV). Lastly, the remarkable metal conductivity of Ti 3 C 2 MXene ensures efficient electron transfer, thereby enhancing overall sensing performance.

Topics & Concepts

Materials scienceNanostructureCrystallographyNanotechnologyChemistryMXene and MAX Phase Materials2D Materials and ApplicationsGas Sensing Nanomaterials and Sensors