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Visible-Light-Induced Difluoroalkylated Cyclization of Novel Functionalized Aromatic Isocyanides

Yingke Feng, He Wang, Mengxing Cui, Ran Sun, Xin Wang, Chen Yang, Lei Li

2023Chinese Journal of Organic Chemistry12 citationsDOIOpen Access PDF

Abstract

In this study, a visible-light photoredox-catalyzed difluoroalkylation of newly designed functionalized aromatic isocyanides with commercially available CF2 precursors was reported.A series of CF2-containing indole-1,2-fused diazepanones were constructed in cascade reaction through a sequence of radical addition/cyclization processes under mild conditions.This reaction not only generated a class of polycyclic indole fused seven-membered nitrogen heterocycles but also expanded the reactions of functionalized isocyanides.

Topics & Concepts

ChemistryCombinatorial chemistryPhotochemistryStereochemistryFluorine in Organic ChemistryRadical Photochemical ReactionsOxidative Organic Chemistry Reactions
Visible-Light-Induced Difluoroalkylated Cyclization of Novel Functionalized Aromatic Isocyanides | Litcius