Litcius/Paper detail

Iron-Catalyzed Borylation of Aryl Ethers via Cleavage of C–O Bonds

Xiaoqin Zeng, Yuxuan Zhang, Zhengli Liu, Shasha Geng, Yun He, Feng Zhang

2020Organic Letters58 citationsDOI

Abstract

Herein, we report the iron-catalyzed borylation of aryl ethers and aryl amines via cleavage of C-O and C-N bonds. This protocol does not require the use of Grignard reagents and displays a broad substrate scope, which allows the late-stage borylation. It also provides facile access to multisubstituted arenes through C-H functionalization using 2-pyridyloxy as the directing group.

Topics & Concepts

BorylationChemistryArylCatalysisCleavage (geology)ReagentCombinatorial chemistryBond cleavageMedicinal chemistrySubstrate (aquarium)Functional groupOrganic chemistryOceanographyEngineeringGeologyAlkylPolymerFracture (geology)Geotechnical engineeringCatalytic C–H Functionalization MethodsCatalytic Cross-Coupling ReactionsOrganoboron and organosilicon chemistry