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Boradigermaallyl: (4+3) Cycloaddition‐Initiated Boron Insertion into Benzene

Ralf H. Kern, Meike Schneider, Klaus Eichele, Hartmut Schubert, Holger F. Bettinger, Lars Wesemann

2023Angewandte Chemie International Edition13 citationsDOIOpen Access PDF

Abstract

The 2π electron 1,3-dipole boradigermaallyl, valence-isoelectronic to an allyl cation, is synthesized from a bis(germylene). It reacts with benzene at room temperature by insertion of a boron atom into the benzene ring. Computational investigation of the mechanism shows the boradigermaallyl reacting with a benzene molecule in a concerted (4+3) or [π4s+π2s] cycloaddition reaction. Thus, the boradigermaallyl acts as a highly reactive dienophile in this cycloaddition reaction with nonactivated benzene as diene unit. This type of reactivity provides a novel platform for ligand assisted borylene insertion chemistry.

Topics & Concepts

CycloadditionBenzeneChemistryBoronPhotochemistryReactivity (psychology)Valence (chemistry)MoleculeMedicinal chemistryRing (chemistry)Organic chemistryCatalysisAlternative medicineMedicinePathologyOrganoboron and organosilicon chemistrySynthesis and characterization of novel inorganic/organometallic compoundsOrganometallic Complex Synthesis and Catalysis
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