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Phase Transitions in Inorganic Halide Perovskites from Machine-Learned Potentials

Erik Fransson, Julia Wiktor, Paul Erhart

2023The Journal of Physical Chemistry C61 citationsDOIOpen Access PDF

Abstract

High Resolution Image Download MS PowerPoint Slide The atomic scale dynamics of halide perovskites have a direct impact not only on their thermal stability but also on their optoelectronic properties. Progress in machine-learned potentials has only recently enabled modeling the finite temperature behavior of these materials using fully atomistic methods with near first-principles accuracy. Here, we systematically analyze the impact of heating and cooling rate, simulation size, model uncertainty, and the role of the underlying exchange-correlation functional on the phase behavior of CsPbX 3 with X = Cl, Br, and I, including both the perovskite and the δ-phases. We show that rates below approximately 60 K/ns and system sizes of at least a few tens of thousands of atoms should be used to achieve convergence with regard to these parameters. By controlling these factors and constructing models that are specific for different exchange-correlation functionals, we then assess the behavior of seven widely used semilocal functionals (LDA, vdW-DF-cx, SCAN, SCAN+rVV10, PBEsol, PBE, and PBE+D3). The models based on LDA, vdW-DF-cx, and SCAN+rVV10 agree well with experimental data for the tetragonal-to-cubic-perovskite transition temperature in CsPbI 3 and also achieve reasonable agreement for the perovskite-to-delta phase transition temperature. They systematically underestimate, however, the orthorhombic-to-tetragonal transition temperature. All other models, including those for CsPbBr 3 and CsPbCl 3, predict transition temperatures below the experimentally observed values for all transitions considered here. Among the considered functionals, vdW-DF-cx and SCAN+rVV10 yield the closest agreement with experiment, followed by LDA, SCAN, PBEsol, PBE, and PBE+D3. Our work provides guidelines for the systematic analysis of dynamics and phase transitions in inorganic halide perovskites and similar systems. It also serves as a benchmark for the further development of machine-learned potentials as well as exchange-correlation functionals.

Topics & Concepts

Perovskite (structure)Tetragonal crystal systemHalideOrthorhombic crystal systemPhase transitionMaterials sciencePhase (matter)Yield (engineering)Chemical physicsThermodynamicsChemistryCrystallographyPhysicsCrystal structureInorganic chemistryMetallurgyOrganic chemistryPerovskite Materials and ApplicationsMachine Learning in Materials ScienceAdvanced Thermoelectric Materials and Devices