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Zinc(II) 2D Coordination Polymer With Terephthalate and 4,6‐Bis(Imidazol‐1‐yl)‐2,1,3‐Benzoxadiazole Linkers as a Selective Luminescent Probe for Gallium(III) Cations

Vladislava V. Matveevskaya, Dmitry I. Pavlov, Alexey A. Ryadun, E. Kh. Sadykov, Tatiana Y. Guselnikova, Vladimir P. Fedin, Xiaolin Yu, Аndrei S. Potapov

2025Applied Organometallic Chemistry9 citationsDOIOpen Access PDF

Abstract

ABSTRACT A two‐dimensional (2D) zinc(II) coordination polymer CP‐1 , [Zn(im 2 bod)(bdc)] n (im 2 bod = 4,6‐bis(imidazol‐1‐yl)‐2,1,3‐benzoxadiazole, bdc 2− = 1,4‐benzenedicarboxylate), was synthesized and fully characterized. CP‐1 crystallizes in the monoclinic crystal system, space group P 2 1 /n. Zn 2+ ions adopt a four‐coordinated distorted tetrahedral geometry. The structure of CP‐1 comprises a two‐dimensional layer consisting Zn 2+ cations connected by im 2 bod and bdc 2− ligands. The adjutant layers participate in π‐π stacking interactions via the benzene and 2,1,3‐benzoxadiazole rings. CP‐1 demonstrated a blue emission with the maximum at 490 nm and a photoluminescence quantum yield 24%. Luminescent sensing properties of CP‐1 in aqueous suspension toward metal cations were evaluated, and selective emission quenching response was observed toward Ga 3+ cations with the limit of detection 10 μM.

Topics & Concepts

ChemistryLuminescenceGalliumZincPolymerCoordination polymerPolymer chemistryInorganic chemistryCombinatorial chemistryOrganic chemistryOptoelectronicsPhysicsMetal-Organic Frameworks: Synthesis and ApplicationsMagnetism in coordination complexesMetal complexes synthesis and properties