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Structure–Activity Relationship for the Catalytic Hydrogenation of Nitrobenzene by Single Platinum Atoms Supported on Nitrogen-Doped Carbon

Caili Wang, Boyong Ye, Ruru Zhou, Yuanyuan Jiang, Zhaoyin Hou

2022ACS Applied Nano Materials29 citationsDOI

Abstract

The preparation of N-doped carbon with well-defined and well-controlled doping of N species is a challenging work, especially with supported Pt atoms. Here, four kinds of N-doped carbons with well-controlled N species were synthesized using Friedel–Crafts reaction or thermal pyrolysis. It was found that the strong interaction between Pt and N in C–N═C and bridged −NH at the edge of heptazine rings in g-C3N4 improved the performance of Pt/g-C3N4 for nitrobenzene hydrogenation. The calculated turnover frequency of each Pt atom in Pt/g-C3N4 reached 42,865 h–1 at 50 °C, and it was stable for five cycles without agglomeration or leaching of Pt species. These findings provide a promising way for the rational design of the hydrogenation catalysts and the development of well-controlled N-doped carbon materials.

Topics & Concepts

NitrobenzeneCatalysisPlatinumCarbon fibersDopingPyrolysisMaterials scienceLeaching (pedology)NitrogenCatalytic hydrogenationInorganic chemistryChemistryOrganic chemistryOptoelectronicsComposite numberComposite materialEnvironmental scienceSoil scienceSoil waterNanomaterials for catalytic reactionsAdvancements in Battery MaterialsAdvanced Photocatalysis Techniques
Structure–Activity Relationship for the Catalytic Hydrogenation of Nitrobenzene by Single Platinum Atoms Supported on Nitrogen-Doped Carbon | Litcius