Changes in the Properties of Different Zones in Multilayered Translucent Zirconia Used in Monolithic Restorations During Aging Process

Abstract

This study assessed the changes in the mechanical and surface properties of the transition zone in multilayered translucent monolithic zirconia subjected to long-term hydrothermal aging. A total of 360 disk-shaped specimens (diameter: 15.0 mm; thickness: 1.2 mm) were prepared using conventional (3Y-TZP in LT; ZL, 4Y-TZP in MT; ZM) and multilayered translucent zirconia (5Y-TZP in MT Multi; ZT, 3Y/5Y-TZP in Prime; ZP) among IPS e.max ZirCAD blocks. Specimens were divided into three groups (n = 30) and aged in the autoclave at 134 °C under 0.2 MPa for 0 h (control group), 5 h (first aged group), and 10 h (second aged group). The mechanical and surface properties of the transition zone in the multilayered translucent zirconia were investigated, followed by statistical analysis (α = 0.05). Before and after aging, ZL (1102.64 ± 41.37 MPa) and ZP (1014.71 ± 139.86 MPa) showed the highest biaxial flexural strength (BFS); ZL showed the highest Weibull modulus (31.46) and characteristic strength (1121.63 MPa); and ZT exhibited the highest nanoindentation hardness (20.40 ± 1.80 GPa) and Young’s modulus (284.90 ± 20.07 GPa). After aging, ZL (116.75 ± 9.80 nm) exhibited the highest surface roughness (Ra); the monoclinic phase contents in ZL and ZP increased; and surface uplifts, microcracks, and irregular defects caused by phase transformation appeared on ZL and ZP surfaces. The 3Y/5Y-TZP transition zone exhibited flexural strength, Vickers hardness, phase distribution changes, and surface microstructure changes similar to those of 3Y-TZP before and after aging; however, the surface roughness was lower than that of 3Y-TZP and higher than those of 4Y-TZP and 5Y-TZP after aging. The mechanical and surface characteristics, excluding BFS and Vickers hardness, were influenced by the yttrium oxide content in each zone and the aging process.

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