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Palladium-Catalyzed Nondirected Late-Stage C–H Deuteration of Arenes

Mirxan Farizyan, Arup Mondal, Sourjya Mal, Fritz Deufel, Manuel van Gemmeren

2021Journal of the American Chemical Society111 citationsDOIOpen Access PDF

Abstract

-acylsulfonamide group. The reported protocol enables high degrees of deuterium incorporation via a reversible C-H activation step and features extraordinary functional group tolerance, allowing for the deuteration of complex substrates. This is exemplified by the late-stage isotopic labeling of various pharmaceutically relevant motifs and related scaffolds. We expect that this method, among other applications, will prove useful as a tool in drug development processes and for mechanistic studies.

Topics & Concepts

ChemistryPalladiumDeuteriumCatalysisDenticityFunctional groupCombinatorial chemistryDrug discoveryStereochemistryComputational chemistryMetalOrganic chemistryBiochemistryPhysicsQuantum mechanicsPolymerChemical Reactions and IsotopesAsymmetric Hydrogenation and CatalysisEpigenetics and DNA Methylation
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