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Palladium-Catalyzed Asymmetric Carbonylation of Alkynes to Axially Chiral Carbothioate Esters

Yao Wang, Yang Yuan, Ting Yang, Yong‐Gui Zhou, Xiao‐Feng Wu

2025Journal of the American Chemical Society18 citationsDOIOpen Access PDF

Abstract

High Resolution Image Download MS PowerPoint Slide Herein, we report a novel palladium-catalyzed asymmetric hydrothioesterification of alkynes under mild conditions, enabling the precise construction of axially chiral carboxylic thioester derivatives with excellent yields, regioselectivity, E / Z selectivity, and enantioselectivity. Disulfides and thiosulfonates were applicable, as well.

Topics & Concepts

ChemistryAxial symmetryCarbonylationThioesterAxial chiralityCarboxylic acidChirality (physics)CatalysisPolymer chemistryCombinatorial chemistryOrganic chemistryMedicinal chemistryDimerComputational chemistryAxial and Atropisomeric Chirality SynthesisCatalytic C–H Functionalization MethodsAsymmetric Synthesis and Catalysis
Palladium-Catalyzed Asymmetric Carbonylation of Alkynes to Axially Chiral Carbothioate Esters | Litcius