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Cu-Catalyzed highly regioselective 1,2-hydrocarboxylation of 1,3-dienes with CO<sub>2</sub>

Penglin Zhang, Zhanglang Zhou, Rumeng Zhang, Qian Zhao, Chun Zhang

2020Chemical Communications25 citationsDOI

Abstract

A practical copper-catalyzed highly regioselective 1,2-hydrocarboxylation of terminal 1,3-diene with carbon dioxide has been developed. Under mild reaction conditions, this chemistry afforded 2-benzyl-β,γ-unsaturated acid derivatives as products, which are a kind of important unit for bio-active molecules and versatile precursors for organic synthesis, with good functional group tolerance. The key intermediate in this transformation is illustrated by control experiments.

Topics & Concepts

RegioselectivityChemistryCatalysisCombinatorial chemistryMedicinal chemistryOrganic chemistryCarbon dioxide utilization in catalysisAsymmetric Hydrogenation and CatalysisCO2 Reduction Techniques and Catalysts